Microplastics with py-GC/MS in sediment, soil, or sludge

Analysis to screen a material for the presence of brominated fire retardants (BFRs), including polybrominated biphenyls (PBBs) and polybrominated diphenyl ethers (PBDEs). The test is performed with a pyrolysis gas-chromatography mass spectrometer (py-GC-MS) according to the ISO 7270-1 standard. The sample is pyrolyzed, which is followed by separation and identification with GC-MS. The obtained pyrogram is then compared to a blank sample that does not contain any brominated fire retardants. We also offer the analysis for electrotechnical products as per IEC 62321-6. Please ask our experts for more information about this option.

Determination of vitamin B7 (biotin) in food with an HPLC-UV-VIS method, or in supplements with a UPLC-MS/MS method. According to Regulation (EU) No 1169/2011, the biotin content of food products may be included in the nutrition declaration if it is present in significant amounts. The daily reference intake for biotin is 50 µg, and biotin content can be declared if the product contains at least: 7.5 µg/100 g or 100 ml in products other than beverages (15% of reference intake), 3.75 µg/100 ml in beverages (7.5% of reference intake), 7.5 µg per portion if the package contains a single portion (15% of reference intake). Foods that contain at least the above amounts of biotin can be labeled with the nutrition claim "Source of biotin." Additional nutrition and health claims related to vitamin B7 can be applied in accordance with Regulations (EC) No 1924/2006 and (EU) No 432/2012.

This metal screening analysis includes the semi-quantitative determination of 70 elements. The method can be used, for example, to determine the background concentrations of metals in environmental samples or to study the elemental distribution of unknown samples. Screening is also often performed to assess which metals should be analyzed by a quantitative method. The measurement is performed using a high-resolution ICP-MS technique (ICP-SFMS), which can identify very low elemental concentrations. A semi-quantitative determination of the following elements is included: Ag, Al, As, Au, B, Ba, Be, Bi, Br, Ca, Cd, Ce, Co, Cr, Cs, Cu, Dy, Er, Eu, Fe, Ga, Gd, Ge, Hf, Hg, Ho, I, Ir, K, La, Lu, Mg, Mn, Mo, Na, Nb, Nd, Ni, Os, P, Pb, Pd, Pr, Pt, Rb, Re, Rh, Ru, S, Sb, Sc, Se, Si, Sm, Sn, Sr, Ta, Tb, Te, Th, Ti, Tl, Tm, U, V, W, Y, Yb, Zn and Zr. However, please note that some elements may not be determinable due to matrix interference. During this semi-quantitative analysis, the instrument is calibrated for about 30 elements and the rest of the analytes are quantified using sensitivity factors for calibrated elements with similar mass and first ionization potential considering isotope abundances. Quantitative analysis is also available at an additional price. During this analysis, all elements are calibrated (excluding halogens and Os). Please ask for an offer for this service.

Determination of vitamin B2 (riboflavin) in food with an HPLC-MS/MS method, or in dietary supplements with a UPLC-MS/MS method. According to Regulation (EU) No 1169/2011, the daily reference intake for riboflavin is 1.4 mg. Riboflavin content may be included in the nutrition declaration if it is present in food products in at least the following amounts: 210 µg/100 g or 100 ml in products other than beverages (15% of reference intake), 105 µg/100 ml in beverages (7.5% of reference intake), 210 µg per portion if the package contains a single portion (15% of reference intake). Foods and beverages that contain at least the above amounts of riboflavin can be labeled with the nutrition claim "Source of riboflavin." Some of the health claims applicable to such products include the following: "Riboflavin contributes to normal energy-yielding metabolism", "Riboflavin contributes to the maintenance of normal skin", "Riboflavin contributes to normal functioning of the nervous system", "Riboflavin contributes to the reduction of tiredness and fatigue".

Determination of Be, Ba, Co, Al, Mg, Cu, Li, Mn, Ag, Sn, Ti, V, Zn, Tl, B, Hg, Mo, Fe, Ca, K, U, P, Cd, Na, Cr, Ni, Pb, Sb, As, and Se in water samples with ICP-MS-technique. The sample is homogenized and acidified (HNO3), after which the analysis is performed from the liquid phase. The analysis is suitable for natural waters. If the sample contains a lot of solids or the matrix is significantly different from natural water (for example waste and industrial waters), please contact our testing expert and ask for an offer. The concentration of each element is reported in µg/l.

Determination of vitamin B1 (thiamine) in food with an HPLC-MS/MS method, or in dietary supplements with a UPLC-MS/MS method. According to Regulation (EU) No 1169/2011, thiamine content may be included in the nutrition declaration for food products if it is present in significant amounts. Considering the daily reference intake (DRI) of 1.1 mg, thiamin can be declared in at least the following amounts: 165 µg/100 g or 100 ml in products other than beverages (15% of DRI), 82.5 µg/100 ml in beverages (7.5% of DRI), 165 µg per portion if the package contains a single portion (15% of DRI). Foods and beverages that contain at least the above amounts of thiamine are considered sources of thiamine. Such products may be labeled with additional health claims, such as: Thiamine contributes to normal energy-yielding metabolism, Thiamine contributes to normal functioning of the nervous system, Thiamine contributes to the normal function of the heart, Thiamine contributes to normal psychological function. More information on permitted nutrition and health claims can be found in Regulations (EC) No 1924/2006 and (EU) No 432/2012.

This PFAS analysis covers the 20 compounds listed in Directive (EU) 2020/2184 (the New Drinking Water Directive) under the parameter "Sum of PFAS". The sum of these compounds should not exceed 0.10 μg/l. Compound (Abbreviation) Perfluorobutanoic acid (PFBA) Perfluoropentanoic acid (PFPA) Perfluorohexanoic acid (PFHxA) Perfluoroheptanoic acid (PFHpA) Perfluorooctanoic acid (PFOA) Perfluorononanoic acid (PFNA) Perfluorodecanoic acid (PFDA) Perfluoroundecanoic acid (PFUnDA) Perfluorododecanoic acid (PFDoDA) Perfluorotridecanoic acid (PFTrDA) Perfluorobutane sulfonic acid (PFBS) Perfluoropentane sulfonic acid (PFPS) Perfluorohexane sulfonic acid (PFHxS) Perfluoroheptane sulfonic acid (PFHpS) Perfluorooctane sulfonic acid (PFOS) Perfluorononane sulfonic acid (PFNS) Perfluorodecane sulfonic acid (PFDS) Perfluoroundecane sulfonic acid Perfluorododecane sulfonic acid Perfluorotridecane sulfonic acid

Determination of PFAS compounds using a method based on the US EPA 1633. Wide analysis package including the following 49 PFAS-compounds: Compound Abbreviation CAS number Perfluorobutanoic acid PFBA 375-22-4 Perfluoropentanoic acid PFPeA 2706-90-3 Perfluorohexanoic acid PFHxA 307-24-4 Perfluoroheptanoic acid PFHpA 375-85-9 Perfluorooctanoic acid PFOA 335-67-1 Perfluorononanoic acid PFNA 375-95-1 Perfluorodecanoic acid PFDA 335-76-2 Perfluoroundecanoic acid PFUnA 2058-94-8 Perfluorododecanoic acid PFDoA 307-55-1 Perfluorotridecanoic acid PFTrDA 72629-94-8 Perfluorotetradecanoic acid PFTeDA 376-06-7 Perfluorobutanesulfonic acid PFBS 375-73-5 Perfluoropentansulfonic acid PFPeS 2706-91-4 Perfluorohexanesulfonic acid PFHxS 355-46-4 Perfluoroheptanesulfonic acid PFHpS 375-92-8 Perfluorooctanesulfonic acid PFOS 1763-23-1 Perfluorononanesulfonic acid PFNS 68259-12-1 Perfluorodecanesulfonic acid PFDS 335-77-3 Perfluorododecanesulfonic acid PFDoS 79780-39-5 1H,1H, 2H, 2H-Perfluorohexane sulfonic acid 4:2FTS 757124-72-4 1H,1H, 2H, 2H-Perfluorooctane sulfonic acid 6:2FTS 27619-97-2 1H,1H, 2H, 2H-Perfluorodecane sulfonic acid 8:2FTS 39108-34-4 Perfluorooctanesulfonamide PFOSA 754-91-6 N-methyl perfluorooctanesulfonamide NMeFOSA 31506-32-8 N-ethyl perfluorooctanesulfonamide NEtFOSA 4151-50-2 N-methyl perfluorooctanesulfonamidoacetic acid NMeFOSAA 2355-31-9 N-ethyl perfluorooctanesulfonamidoacetic acid NEtFOSAA 2991-50-6 N-methyl perfluorooctanesulfonamidoethanol NMeFOSE 24448-09-7 N-ethyl perfluorooctanesulfonamidoethanol NEtFOSE 1691-99-2 Hexafluoropropylene oxide dimer acid HFPO-DA 13252-13-6 4,8-Dioxa-3H-perfluorononanoic acid ADONA 919005-14-4 Perfluoro-3-methoxypropanoic acid PFMPA 377-73-1 Perfluoro-4-methoxybutanoic acid PFMBA 863090-89-5 Nonafluoro-3,6-dioxaheptanoic acid NFDHA 151772-58-6 9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid 9Cl-PF3ONS 756426-58-1 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid 11Cl-PF3OUdS 763051-92-9 Perfluoro(2-ethoxyethane)sulfonic acid PFEESA 113507-82-7 3-Perfluoropropyl propanoic acid 3:3FTCA 356-02-5 2H,2H,3H,3H-Perfluorooctanoic acid 5:3FTCA 914637-49-3 3-Perfluoroheptyl propanoic acid 7:3FTCA 812-70-4 Perfluoroethylcyclohexane sulfonate PFecHS 335-24-0 1H,1H,2H,2H-Perfluorododecanesulfonate 10:2 FTS 108026-35-3 Perfluorobutane sulfonamide FBSA 30334-69-1 Perfluorohexanesulfonamide FHxSA 41997-13-1 Perfluorooctane sulfonamidoacetic acid FOSAA 2806-24-8 Perfluoro-2,5-dimethyl-3,6-dioxanonanoic acid HFPO-TA 13252-14-7 Perfluorohexadecanoic acid PFHxDA 67905-19-5 Perfluorooctadecanoic acid PFODA 16517-11-6 Perfluoroundecanesulfonic acid PFUnDS 749786-16-1 Please contact our experts through the form below for more detailed information on the analysis.

ICP-OES measurement package for soil, sludge, or sediment samples. Pre-treatment of the sample with aqua regia decomposition is included in the price. The following elements are quantified using the ICP-OES technique: Ag, As, Ba, Be, Cd, Co, Cr, Cu, Fe, Hg, Li, Mn, Mo, Ni, Pb, Sb, Sn, Sr, Tl, V, and Zn. The concentrations are expressed in mg/kg d.m. The analysis is also available with an express turnaround time. Ask our experts for more information.

Determination of carbon, hydrogen, nitrogen, sulfur, and oxygen content of an organic sample. CHNS analysis (”LECO analysis”) is performed using a flash combustion method, where the sample is combusted under 25 kPa of O2 at an elevated temperature (1000 °C), followed by gas chromatography separation and detection using a thermal conductivity detector. Oxygen is analyzed by reduction on granulated carbon at 1480 °C, utilizing high-temperature thermal decomposition and conversion of oxygen into carbon monoxide before gas chromatography separation and detection with a thermal conductivity detector. The sample can be either solid or liquid, but water in the sample affects the results. In the case of aqueous samples, it is possible to dry the sample before analysis. The price includes two parallel measurements. The results are reported as wt-% of the initial sample. The ash, drying and dry loss measurements will increase the minimum required sample material need to 300 mg. The analysis gives the total carbon, hydrogen, nitrogen, sulfur, and oxygen content of the material, but it does not identify any chemical structures. The measurement can be combined with other methods, such as GC-MS, 1H, and 13C NMR, to perform substance structure identification. Possible element packages: O, CHNS, and CHNOS.