ICP-OES Heavy metals quantification of soil, sludge or sediment (As, Cd, Co, Cr, Cu, Hg, Ni Pb, Sb, V and Zn)

ICP-OES measurement package for soil, sludge, or sediment samples. Pre-treatment of the sample with aqua regia decomposition is included in the price. The following elements are quantified using the ICP-OES technique: Ag, As, Ba, Be, Cd, Co, Cr, Cu, Fe, Hg, Li, Mn, Mo, Ni, Pb, Sb, Sn, Sr, Tl, V, and Zn. The concentrations are expressed in mg/kg d.m. The analysis is also available with an express turnaround time. Ask our experts for more information.

Nutrient measurement package for soil, sludge, or sediment samples using the ICP-OES method. The price of the analysis includes the pre-treatment of the sample with aqua regia decomposition and the measurement of the following elements using the ICP-OES technique: Al, B, Bi, Ca, K, Mg, Na, S, Se, Si, Te, Ti, and Zr. The concentrations of the measured elements are expressed in mg/kg d.m. The analysis is also available with express delivery time. Ask for an offer from our expert.

This metal screening analysis includes the semi-quantitative determination of 70 elements. The method can be used, for example, to determine the background concentrations of metals in environmental samples or to study the elemental distribution of unknown samples. Screening is also often performed to assess which metals should be analyzed by a quantitative method. The measurement is performed using a high-resolution ICP-MS technique (ICP-SFMS), which can identify very low elemental concentrations. A semi-quantitative determination of the following elements is included: Ag, Al, As, Au, B, Ba, Be, Bi, Br, Ca, Cd, Ce, Co, Cr, Cs, Cu, Dy, Er, Eu, Fe, Ga, Gd, Ge, Hf, Hg, Ho, I, Ir, K, La, Lu, Mg, Mn, Mo, Na, Nb, Nd, Ni, Os, P, Pb, Pd, Pr, Pt, Rb, Re, Rh, Ru, S, Sb, Sc, Se, Si, Sm, Sn, Sr, Ta, Tb, Te, Th, Ti, Tl, Tm, U, V, W, Y, Yb, Zn and Zr. However, please note that some elements may not be determinable due to matrix interference. During this semi-quantitative analysis, the instrument is calibrated for about 30 elements and the rest of the analytes are quantified using sensitivity factors for calibrated elements with similar mass and first ionization potential considering isotope abundances. Quantitative analysis is also available at an additional price. During this analysis, all elements are calibrated (excluding halogens and Os). Please ask for an offer for this service.

Determination of Be, Ba, Co, Al, Mg, Cu, Li, Mn, Ag, Sn, Ti, V, Zn, Tl, B, Hg, Mo, Fe, Ca, K, U, P, Cd, Na, Cr, Ni, Pb, Sb, As, and Se in water samples with ICP-MS-technique. The sample is homogenized and acidified (HNO3), after which the analysis is performed from the liquid phase. The analysis is suitable for natural waters. If the sample contains a lot of solids or the matrix is significantly different from natural water (for example waste and industrial waters), please contact our testing expert and ask for an offer. The concentration of each element is reported in µg/l.

Determination of carbon, hydrogen, nitrogen, sulfur, and oxygen content of an organic sample. CHNS analysis (”LECO analysis”) is performed using a flash combustion method, where the sample is combusted under 25 kPa of O2 at an elevated temperature (1000 °C), followed by gas chromatography separation and detection using a thermal conductivity detector. Oxygen is analyzed by reduction on granulated carbon at 1480 °C, utilizing high-temperature thermal decomposition and conversion of oxygen into carbon monoxide before gas chromatography separation and detection with a thermal conductivity detector. The sample can be either solid or liquid, but water in the sample affects the results. In the case of aqueous samples, it is possible to dry the sample before analysis. The price includes two parallel measurements. The results are reported as wt-% of the initial sample. The ash, drying and dry loss measurements will increase the minimum required sample material need to 300 mg. The analysis gives the total carbon, hydrogen, nitrogen, sulfur, and oxygen content of the material, but it does not identify any chemical structures. The measurement can be combined with other methods, such as GC-MS, 1H, and 13C NMR, to perform substance structure identification. Possible element packages: O, CHNS, and CHNOS.

Determination of total fluorine (F) content in plastic according to the EN 15408 mod. method. The fluorine content of the sample is obtained using oxygen bomb combustion treatment followed by ion chromatography (IC). Possible sample preparation, such as grinding into smaller particles, is available at an extra cost. This method can also be used to determine the total content of S, Cl, and Br. The results will be reported in mg/kg.

Determination of Sb, As, Hg, Cd, Co, Cr, Cu, Pb, Ni, Zn, and V from water samples with the ICP-MS technique. The concentration of each element is expressed in µg/l.

The measurement determines the content of dissolved silicon in ultrapure water using UV-Vis spectroscopy (molybdenum heteropolyblue method). The silicon detection limit is 0.7 ppb. The sample must be collected in a suitable sample container designed for ultrapure water. Measurlabs can provide the required sample vessels upon request.

Determination of 36 elemental impurities from ultra-pure water with ICP-MS. The measurement includes the following elements: Al, Sb, As, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, Ge, Au, Fe, Pb, Li, Mg, Mn, Mo, Ni, Nb, Pt, K, Ag, Na, Sr, Ta, Tl, Sn, Ti, W, V, Zn, and Zr. The sample must be collected in a suitable container designed for ultrapure water. Measurlabs can provide the required sample vessels.

Quantitative mineralogical analysis by X-ray powder diffraction (XRD) on bentonite samples to identify and quantify the concentration of occurring minerals. The analysis is performed according to EN 13925. The results of the analysis are expressed as percentages, for example: % of Smectite, % of Quartz, % of Calcite, % of Opal, % of Feldspar. The uncertainty of the measurement is 10–20%.