Polymer characterization by NMR
NMR can be used to identify the type(s) of polymer(s) in a sample by studying the unique response of their nuclei to an applied magnetic field. This technique can be used to characterize a completely unknown polymer or a blend of polymers.
NMR can also be used to study the purity or contamination of a polymer sample. During polymer synthesis, compounding, or manufacturing, materials can become mixed with unwanted polymers or other organic contaminants. NMR can identify these molecules and quantify their concentration in the sample relative to the intended polymer composition.
The processed spectrum is delivered as an image file. Additional interpretation and raw data can be provided upon request.
Please contact Measurlabs' NMR experts to receive a testing plan tailored to your material and analysis needs. 1H-NMR and/or 13C-NMR may be used for this analysis based on the sample. Solid-state measurements are also available.
The price of the measurement can depend on whether your samples require the use of specialized deuterated solvents or measurement conditions (i.e. high temperatures or long measurement times).
More information about the method:
NMR spectroscopy- Suitable sample matrices
- Polymers soluble in deuterated solvent. Solid-state measurements are also available.
- Required sample quantity
- ~100 mg
- Typical turnaround time
- 3 weeks after receiving the samples
- Detection limit
- Accurate in identifying the presence of molecular groups to a concentration of ~1%.
- Available quality systems
- Measurlabs validated method
- Device types
- Method expert
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