Residual peroxides in silicone
The general requirement in Section III of German BfR recommendation XV for silicones states that:
The finished products must not test positively for peroxides.
Test method according to 58. Mitteilung zur Untersuchung von Kunststoffen: Bundesgesundheitsblatt 40, (1997).
- Suitable sample matrices
- Plastic, rubber, silicone, elastomers, childcare articles
- Required sample quantity
- 50 g
- Typical turnaround time
- 4 weeks after receiving the samples
- Available quality systems
- Accredited test method
- Method expert
Price
Typical price range (Excl. VAT):
180–245 €per sample
We also charge a 97 € service fee per order.
Large batches of samples are eligible for discounts.
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Other tests we offer
Release of N-nitrosamines and N-nitrosable substances
EN 12868 (mod.), EN 14350
N-nitrosamines and N-nitrosatable substances are present, usually in trace quantities, in various environmental media, certain food products, cosmetics, and rubber products. In particular, those found in rubber products are thought to originate from certain additives used in the vulcanization of rubber. Regulatory reference / standard Applicable materials Compliance limits Applicable reference method Commission Directive 93/11/EEC Elastomer or rubber teats and soothers N-nitrosamines released: 0.01 mg/kg N-nitrosatable substances released: 0.1 mg/kg EN 12868 EN 14350 Drinking accessories made of rubber and other elastomers BfR recommendation XXI/1 Commodities based on natural and synthetic rubber in contact with food N-nitrosamines: not detected above 1 µg/dm2 (sum of substances) - N-nitrosamines and N-nitrosatable substances are controlled by Commission Directive 93/11/EEC. In addition, recommendation XXI by Germany’s Federal Institute for Risk Assessment (BfR) has set the migration limit of N-nitrosamines from elastomers to food at ≤ 1.0 µg/dm2. The test package covers analysis of the release of the following N-nitrosamines (free and after nitrosation) into artificial saliva simulant or a food simulant: Substance Abbreviation CAS No N-Nitrosodimethylamine NDMA 62-75-9 N-Nitrosodi-n-propylamine NDPA 621-64-7 N-Nitrosodi-n-butylamine NDBA 924-16-3 N-Nitrosopiperidine NPIP 100-75-4 N-Nitrosopyrrolidine NPYR 930-55-2 N-Nitrosomorpholine NMOR 59-89-2 N-Nitrosobenzylamine NDBzA 937-32-6 N-Nitrosodi-n-amylamine NDiNA 2050-92-2 N-Nitroso-methylphenylamine NMPhA 937-35-9 N-Nitrosoethylphenylamine NEPhA 612-64-6
268 €
Read moreContent of volatile matter in silicone elastomers
EN 14350, EN 14372
Accredited laboratory analysis for determining the amount of volatile organic matter in silicone used in food contact materials or childcare articles. Testing can be conducted according to the following methods and references: Applicable materials Drying phase Treatment phase Compliance limit Test method Reference General food contact materials made from silicone elastomer 1 h / 100 °C 4 h / 200 °C ≤ 0.5 % Bestimmung von flüchtigen Verbindungen in Bedarfsgegenständen aus Silikon (version 02, 09/2023) BfR XV. Silicones (as of 01.08.2024) Childcare articles intended for drinking 1 h / 100 °C 4 h / 200 °C ≤ 0.5 % EN 14350, art 8.4.2 EN 14350 Childcare articles intended for feeding 1 h / 100 °C 4 h / 200 °C ≤ 0.5 % EN 14372, art. 6.3.3 EN 14372
180–254 €
Read morePolycyclic aromatic hydrocarbons (PAH) in plastic and rubber (AfPS GS 2019:01 PAK)
AfPS GS2019
Content of 15 polycyclic aromatic hydrocarbons (PAHs) in plastic and rubber and products made from them (e.g., toys, kitchenware) according to AfPS GS 2019:01 PAK. If PAH levels are sufficiently low, the product may be granted a GS mark (a voluntary German product safety label). The test package includes the following substances: Naphthalene [CAS: 91-20-3], Acenaphthylene [CAS: 208-96-8] , Acenaphthene [CAS: 83-32-9] , Fluorene [CAS: 86-73-7] , Phenanthrene [CAS: 85-01-8] , Anthracene [CAS: 120-12-7] , Fluoranthene [CAS: 206-44-0] , Pyrene [CAS: 129-00-0] , Benzo(a)anthracene [CAS: 56-55-3] , Chrysene [CAS: 218-01-9] , Benzo(b)fluoranthene [CAS: 205-99-2] , Benzo(k)fluoranthene [CAS: 207-08-9] , Benzo(j)fluoranthene [CAS: 205-82-3] , Benzo(e)pyrene [CAS: 192-97-2] , Benzo(a)pyrene [benzo(def)chrysene] [CAS: 50-32- 8] , Indeno(1,2,3-cd)pyrene [CAS: 193-39-5] , Dibenzo(a,h)anthracene [CAS: 53-70-3] , Benzo(g,h,i)perylene [CAS: 191-24-2].
226 €
Read moreBisphenol A content
CEN/TS 13130-13, EN 14350-2, EN 14372, …
Content of bisphenol A (BPA) in various matrices, including: Consumer goods made from plastic, elastomers, and rubber, Toys and childcare articles, Food packaging (plastic, paper, multi-materials). Extraction is possible with various techniques, including: Cold water extract (EN 645), hot water extract (EN 647), or solvent extract (EN 15519) from packaging containing recycled fibers for compliance according to German BfR recommendation XXXVI, Acetonitrile extract of food contact materials for compliance according to French regulation LOI n° 2012-1442, Release into aqueous simulant from child care articles for compliance according to EN 14372 and EN 14350, Release into aqueous simulant from toys for compliance according to Toy Safety Directive 2009/48/EC. For food contact materials, we also offer a low LOD method that meets the 1 μg/kg detection limit specified in Commission Regulation (EU) 2024/3190. Our experts are happy to provide a quote for BPA testing with this method.
254 €
Read moreBisphenol A, B, F, S, and AF content
Analysis package for quantifying the following bisphenol compounds: bisphenol A (BPA) [CAS: 80-05-7], bisphenol B (BPB) [CAS: 77-40-7], bisphenol F (BPF) [CAS: 620-92-8], bisphenol S (BPS) [CAS: 80-09-1], bisphenol AF (BPAF) [CAS: 1478-61-1]. Testing is primarily intended for: Analyzing recycled PE, PP and LDPE intended for cosmetic packaging according to CosPaTox guidelines, Evaluating the compliance of plastics, paper, and board according to food contact regulations (by modeling migration based on the content). If the analysis is intended for food contact compliance, a method with a lower LOQ (0.05 mg/kg) can be used. Please let us know the goal of the analysis when requesting a quote.
330–498 €
Read moreCyclosiloxanes content
Cyclosiloxanes are the primary building blocks of siloxane polymers and, ultimately, silicone rubber. Hence, cyclosiloxanes can remain in the final silicone article as residual impurities. Several cyclosiloxanes (D4, D5, D6; see table below) are considered harmful to the environment and human health. These three substances are listed in the REACH Candidate List of substances of very high concern (SVHC). Substance Abbreviation CAS N:o Octamethylcyclotetrasiloxane D4 556-67-2 Decamethylcyclopentasiloxane D5 541-02-6 Dodecamethylcyclohexasiloxane D6 540-97-6 The Nordic Swan Ecolabel criteria for greaseproof paper sets the limit values for D4, D5, and D6 impurities in silicone coating as 400 ppm per substance and 1000 ppm for the sum of D4, D5, and D6. In addition to the restricted substances listed above, this analysis package includes the quantification of cyclosiloxanes D3, D7, and D8.
451 €
Read morePolycyclic aromatic hydrocarbons (PAH) - REACH compliance
Analysis of PAH compounds in plastic, rubber, paper, board, and products made from these raw materials (e.g., textiles, toys, packaging materials) as required by the REACH Regulation. Test package includes the following substances: Benzo(a)pyrene [benzo(def)chrysene] [CAS: 50-32-8] , Benzo(e)pyrene [CAS: 192-97-2] , Benzo(a)anthracene [CAS: 56-55-3] , Chrysene [CAS: 218-01-9] , Benzo(b)fluoranthene [CAS: 205-99-2] , Benzo(j)fluoranthene [CAS: 205-82-3] , Benzo(k)fluoranthene [CAS: 207-08-9], Dibenzo(a,h)anthracene [CAS: 53-70-3].
184 €
Read moreAromatic amines derived from azo dyes
EN 14362-1
Determination of certain aromatic amines derived from azo dyes in accordance with the standard EN 14362-1.
369 €
Read moreSpecific migration testing – Uvitex OB
EN 13130-1
Analysis to determine the specific migration of fluorescent whitening agent 2,5-bis(5-tert-butyl-2-benzoxazolyl)thiophene, known by the trade name Uvitex OB [CAS: 7128-64-5], from a sample or material intended for food contact. The substance is listed under FCM 500 and Ref No. 38560 in European Commission Regulation No 2011/10 on plastic food contact materials. The specific migration limit (SML) for Uvitex OB is 0.6 mg/kg of food.
200–295 €
Read moreChildren's cutlery and feeding utensils – Physical and mechanical properties by EN 14372
EN 14372
Test to determine the mechanical and physical properties and safety of cutlery and feeding utensils intended for children from 0 to 48 months of age. The method is based on the EN 14372 standard.
650 €
Read more”Measurlabs was extremely helpful in all our requests during the preceding months. When we had high time pressure to get analytical support, they handled all our requests swiftly. Whenever we have future analytical needs we will remember their excellent service.”
Erich Seger, H.B. Fuller Deutschland GmbH
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